A new methodology was developed to characterize and to quantify the polymer content in PBX (HMX/Viton) by Fourier Transform Infrared Spectroscopy (FT-IR), using the Termogravimetric analysis (TG) as reference techniques for the quantitative method. The quantification methodology, proposed by us, using the Fourier transform infrared-attenuated total reflectance (FT-IR/ATR) showed excellent results, being faster than the usual methodologies and can eliminate the generation of chemical residues.
